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자연과학대학
화학·나노과학전공
Journal papers
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Synthesis of azines in solid state: Reactivity of solid hydrazine with aldehydes and ketones
Title
Synthesis of azines in solid state: Reactivity of solid hydrazine with aldehydes and ketones
Authors
Lee B.
;
Hyung Lee K.
;
Cho J.
;
Nam W.
;
Hur N.H.
Ewha Authors
남원우
;
조재흥
SCOPUS Author ID
남원우
; 조재흥
Issue Date
2011
Journal Title
Organic Letters
ISSN
1523-7060
Citation
Organic Letters vol. 13, no. 24, pp. 6386 - 6389
Indexed
SCI; SCIE; SCOPUS
Document Type
Article
Abstract
Highly conjugated azines were prepared by solid state grinding of solid hydrazine and carbonyl compounds such as aldehydes and ketones, using a mortar and a pestle. Complete conversion to the azine product is generally achieved at room temperature within 24 h, without using solvents or additives. The solid-state reactions afford azines as the sole products with greater than 97% yield, producing only water and carbon dioxide as waste. © 2011 American Chemical Society.
DOI
10.1021/ol202593g
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