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Synthesis of azines in solid state: Reactivity of solid hydrazine with aldehydes and ketones

Title
Synthesis of azines in solid state: Reactivity of solid hydrazine with aldehydes and ketones
Authors
Lee B.Hyung Lee K.Cho J.Nam W.Hur N.H.
Ewha Authors
남원우조재흥
SCOPUS Author ID
남원우scopus
Issue Date
2011
Journal Title
Organic Letters
ISSN
1523-7060JCR Link
Citation
vol. 13, no. 24, pp. 6386 - 6389
Indexed
SCI; SCIE; SCOPUS WOS scopus
Abstract
Highly conjugated azines were prepared by solid state grinding of solid hydrazine and carbonyl compounds such as aldehydes and ketones, using a mortar and a pestle. Complete conversion to the azine product is generally achieved at room temperature within 24 h, without using solvents or additives. The solid-state reactions afford azines as the sole products with greater than 97% yield, producing only water and carbon dioxide as waste. © 2011 American Chemical Society.
DOI
10.1021/ol202593g
Appears in Collections:
자연과학대학 > 화학·나노과학전공 > Journal papers
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