Full metadata record
DC Field | Value | Language |
---|---|---|
dc.contributor.author | 이윤실 | * |
dc.date.accessioned | 2016-08-28T12:08:58Z | - |
dc.date.available | 2016-08-28T12:08:58Z | - |
dc.date.issued | 2010 | * |
dc.identifier.issn | 0009-5893 | * |
dc.identifier.other | OAK-7115 | * |
dc.identifier.uri | https://dspace.ewha.ac.kr/handle/2015.oak/221222 | - |
dc.description.abstract | Melatonin is synthesized from acetylserotonin, which is a deacetylated product of serotoinin. Simultaneous analysis of melatonin and its precursors in rat urine was performed using their (N,O)-ethoxycarbonyl/N-pentafluoropropionyl (EOC/PFP) derivatives by gas chromatography-mass spectrometry (GC-MS). The mass spectral data of acetylserotonin as mono-O-EOC/mono-N-PFP and serotonin as di-(N,O)-EOC/di-N-PFP derivatives were newly established. This method exhibited good linearity (r ≥ 0.996), repeatability (% relative standard deviation = 6.9-9.4), accuracy (% relative error = -8.9 to 8.6) with detection limits of 0.005 to 0.03 ng mL-1. This method was developed for the simultaneous measurement of melatonin and its precursors in rat urine. © 2010 Vieweg+Teubner Verlag | Springer Fachmedien Wiesbaden GmbH. | * |
dc.language | English | * |
dc.title | Simultaneous GC-MS analysis of melatonin and its precursors as ethoxycarbonyl/pentafluoropropionyl derivatives in rat urine | * |
dc.type | Article | * |
dc.relation.issue | 41590 | * |
dc.relation.volume | 72 | * |
dc.relation.index | SCI | * |
dc.relation.index | SCIE | * |
dc.relation.index | SCOPUS | * |
dc.relation.startpage | 1213 | * |
dc.relation.lastpage | 1217 | * |
dc.relation.journaltitle | Chromatographia | * |
dc.identifier.doi | 10.1365/s10337-010-1771-y | * |
dc.identifier.wosid | WOS:000285099500028 | * |
dc.identifier.scopusid | 2-s2.0-78651303868 | * |
dc.author.google | Paik M.J. | * |
dc.author.google | Nguyen D.T. | * |
dc.author.google | Kim Y.J. | * |
dc.author.google | Shin J.Y. | * |
dc.author.google | Shim W. | * |
dc.author.google | Cho E.Y. | * |
dc.author.google | Yoon J.H. | * |
dc.author.google | Kim K.R. | * |
dc.author.google | Lee Y.S. | * |
dc.author.google | Kim N. | * |
dc.author.google | Park S.W. | * |
dc.author.google | Lee G. | * |
dc.author.google | Ahn Y.H. | * |
dc.contributor.scopusid | 이윤실(17137192000) | * |
dc.date.modifydate | 20240130115944 | * |