Crystal structure of the bioctahedral cluster complex K 6[Re 12CS 17(CN) 6]•2CH 3OH• 10H 2O

Abstract

The cluster complex of K 6[Re 12CS 17(CN) 6]•2CH 3OH•10H 2O composition is separated by recrystallization of the K 6[Re 12CS 17(CN) 6]•20H 2O compound from methanol. The compound crystallizes in hexagonal space group P-6m2 with unit cell parameters: a = 10.9932(14) Å, c = 14.631(4) Å, V = 1531.3(5) Å 3, Z = 1, and d calc = 3.720 g/cm 3. © 2009 Pleiades Publishing, Ltd.